Figure 7 TEM micrographs of silica nanoparticles obtained at different aging times. 3 (a), 5 (b), 6 (c), 7 (d), 8 (e), and 12 h (f). The Fourier transform infrared (FT-IR) spectra of the silica nanoparticles dried at 100°C are shown in Figure 8. The peaks at 1,103, 804, and 488 cm−1 are due to the asymmetric, symmetric, and bending modes of SiO2, respectively. The broad absorption band at 3,402 cm−1 and the peak at 1,466 cm−1 for the sample are due to the -OH groups. The absorption bands observed at 2,924 and 2,853 cm−1 are due to the bending of -CH2 and -CH3 of the CTAB surfactant. EPZ004777 molecular weight The FT-IR spectra show C-H peaks at 2,924 and 2,853

cm−1, clearly indicating the organic modification of the nanoparticle surface and the silica nanoparticle obtained

GSK1838705A in amorphous state. Figure 8 FT-IR spectra of the nanoparticles. In addition, the characteristic peak corresponding to the silica crystalline structure was not clearly observed at 2θ = 22° in the XRD diagrams of Figure 9, indicating that the samples are nearly amorphous. Figure 9 XRD diagram of silica nanoparticle. Conclusions RHA material was successfully synthesized from the abundant Vietnamese rice husk. A new synthetic method for spherical silica nanoparticles using RHA as the silica source and CTAB as the surfactant via the sol–gel technique in water/butanol was investigated. This method is a simple and effective route for preparing ultrafine powders on a nanometer scale and with a homogeneous particle size distribution. The specific surface area is reached at 340 m2/g, and the silica product obtained MycoClean Mycoplasma Removal Kit is amorphous. This leads to the low-cost production of silica nanoparticles for various practical applications such as pollution treatment, nanocomposite materials, etc. Furthermore, using this source for the production of RHA provides a way to solve the waste problem of rice husk pollution in the Mekong Delta of Vietnam. Authors’ information VHL graduated

and received his Bachelor of Science in Organical Chemistry in 2005, and after that, he received his M.S. in Physical Chemistry in 2011 from the University of Science, HoChiMinh City, Vietnam. His research interests selleck include nanomaterials and polymers. CNHT is currently the Vice Dean of the Faculty of Materials Science, University of Science-National University of HoChiMinh City, Vietnam. He graduated with the degree B.S. in Physical Chemistry from the University of Science, HoChiMinh City, Vietnam, in 2004. He received his M.S. in Physico-chemistry of Materials from the University of Maine, Le Mans, France, in 2005 and received his Ph.D. in Materials Science and Engineering from the University of Savoie, Chambéry, France, in 2008. His research interests include polymers, nanocomposites based on polymers, and biodegradable polymers. HHT is an associate professor in the Faculty of Chemistry, University of Science, Vietnam National University in HoChiMinh City, Vietnam.